This search combines search strings from the content search (i.e. "Full Text", "Author", "Title", "Abstract", or "Keywords") with "Article Type" and "Publication Date Range" using the AND operator.
Beilstein J. Org. Chem. 2022, 18, 1203–1209, doi:10.3762/bjoc.18.125
Graphical Abstract
Scheme 1: a) Mechanochemical synthesis of g-PCN from sodium phosphide and trichlorotriazine (previous work [38]) ...
Figure 1: PXRD patterns of g-h-PCN (green) and g-h-PCN300 (teal).
Figure 2: XPS scans of a) C 1s, b) N 1s and c) P 2p for the pre-annealed g-h-PCN and d) C 1s, e) N 1s and f) ...
Figure 3: 31P MAS NMR of a) g-h-PCN and b) g-h-PCN300. Asterisks denote spinning sidebands.
Figure 4: Calculated structures for a) corrugated (edge facing), b) corrugated (single layer), c) layered g-h...
Beilstein J. Org. Chem. 2017, 13, 2160–2168, doi:10.3762/bjoc.13.216
Scheme 1: Milling synthesis of 2,3-diphenylquinoxaline from benzil and ortho-phenylenediamine [40].
Scheme 2: Movement of the milling jar and sample holder under milling conditions.
Figure 1: Time-resolved Raman spectrum for the double condensation of o-phenylenediamine and benzil to form 2...
Figure 2: Section of the time-resolved Raman spectrum for the model mechanochemical reaction conducted at 30 ...
Figure 3: (Left) Estimated contribution of each component for each Raman spectrum over time of the synthesis ...
Figure 4: The effect of milling frequency on the milling condensation of benzil and o-phenylenediamine to for...
Figure 5: The reproducibility of varying milling frequency on the neat mechanochemical condensation of benzil...
Figure 6: The effect of milling frequency on the internal jar temperature measured immediately after reaction...
Beilstein J. Org. Chem. 2017, 13, 1963–1968, doi:10.3762/bjoc.13.191
Scheme 1: Developed syntheses for accessing by mechanochemistry: (a) mPEG–OTs, (b) mPEG–Br, (c) mPEG–SH, (d) ...
Figure 1: 1H NMR of sample mPEG2000–OTs (Table 1, entry 5) in CDCl3 showing mPEG end group shift after tosylation.